Quinoline, 3,7-dichloro-8-(dichloromethyl)-

Quinoline, 3,7-dichloro-8-(dichloromethyl)- - Names and Identifiers

Name	3,7-dichloro-8-dichloro methyl quinoline
Synonyms	3,7-dichloro-8-dichloro methyl quinoline Quinoline, 3,7-dichloro-8-(dichloromethyl)-
CAS	84086-97-5

Quinoline, 3,7-dichloro-8-(dichloromethyl)- - Physico-chemical Properties

Molecular Formula	C10H5Cl4N
Molar Mass	280.97
Melting Point	142-144?C
Storage Condition	2-8℃
Physical and Chemical Properties	Chemical quality The pure product is white crystal, m.p.154 ℃, soluble in ethanol, benzene, chlorobenzene, dichlorobenzene and other organic solvents, slightly soluble in petroleum ether, insoluble in water.
Use	Use 3, 7-dichloro-8-dichloromethylquinoline is an intermediate of the herbicide quinclorac.

Quinoline, 3,7-dichloro-8-(dichloromethyl)- - Nature

storage conditions

Hygroscopic, -20°C Freezer, Under Inert Atmosphere

Last Update：2024-04-10 22:29:15

Quinoline, 3,7-dichloro-8-(dichloromethyl)- - Production method

the preparation method is to add 7-chloro-8-methylquinoline and o-dichlorobenzene in the reaction kettle, add the catalyst azobisisobutyronitrile, raise the temperature, pass chlorine gas, and control the unreacted quinoline by gas chromatography until the content is ≤ 1%. Desolubilization recovers o-dichlorobenzene to obtain a mixture of 3, 7-dichloro-8-chloromethylquinoline and 3, 7-dichloro-8-dichloromethylquinoline.

Last Update：2024-04-10 22:29:15